Influence of granulated rubber from waste tires on ASR expansion, microstructure, and mechanical properties of mortars

Daria Jóźwiak-Niedźwiedzka; Dominik Nowicki; Piotr Denis; Magdalena Osial; Alessandro P. Fantilli

doi:10.7409/rabdim.025.018

Published: 2025-09-22

Vol. 24 No. 3 (2025)

Influence of granulated rubber from waste tires on ASR expansion, microstructure, and mechanical properties of mortars

Daria Jóźwiak-Niedźwiedzka

, Dominik Nowicki

, Piotr Denis

, Magdalena Osial

, Alessandro P. Fantilli

Section: Articles

https://doi.org/10.7409/rabdim.025.018

Abstract

The paper presents the results of research on the effect of partially replacing the sand fraction in cement mortar mixes with granulated rubber (GR) from waste tires on the potential for alkali–silica reaction (ASR) occurrence. ASR is a significant durability issue in cement-based composites, which can lead to substantial expansion and cracking in these materials. The study also analyzed the influence of rubber aggregate on the mechanical properties of mortars, particularly compressive and flexural strength, as well as on the microstructure of the mortars. Additionally, the impact of NaOH on the properties of granulated rubber aggregate was evaluated. Reference mortars were prepared using moderately reactive sand (R1) and highly reactive sand (R3), while in the experimental mixes, rubber aggregate was used as a volumetric replacement for a specific sand fraction at levels of 15% and 30%. ASR-related expansion tests were conducted in accordance with the RILEM AAR-2 guidelines. The results showed that partially replacing sand with rubber aggregate effectively reduced ASR-induced expansion, likely due to the rubber’s ability to absorb stress and restrict moisture migration, thereby mitigating the reaction. However, the use of rubber aggregate also led to a decrease in both compressive and flexural strength, which is a typical effect when introducing elastic materials, such as rubber, into cementitious mixes. The findings highlight the potential of granulated rubber from waste tires recycled as a sustainable additive in cement-based materials to control ASR, especially in structures exposed to aggressive environmental conditions. Additionally, the use of this type of aggregate aligns with the principles of the circular economy by utilizing rubber waste and simultaneously delivering both environmental and performance benefits.

Keywords:

ASR, durability, internal structure, rubber aggregate, waste tire

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Jóźwiak-Niedźwiedzka, D., Nowicki, D., Denis, P., Osial, M., & Fantilli, A. P. (2025). Influence of granulated rubber from waste tires on ASR expansion, microstructure, and mechanical properties of mortars. Roads and Bridges – Drogi I Mosty, 24(3), 319–330. https://doi.org/10.7409/rabdim.025.018

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References

Salehi S., Arashpour M., Kodikara J., Guppy R.: Sustainable pavement construction: A systematic literature review of environmental and economic analysis of recycled materials. Journal of Cleaner Production, 313, 2021, Article ID: 127936, DOI: 10.1016/j.jclepro.2021.127936 DOI: https://doi.org/10.1016/j.jclepro.2021.127936
Google Scholar

Liu N., Wang Y., Bai Q., Liu Y., Wang (Slade) P., Xue S., Yu Q., Li Q.: Road life-cycle carbon dioxide emissions and emission reduction technologies: A review. Journal of Traffic and Transportation Engineering (English Edition), 9, 4, 2022, 532-555, DOI: 10.1016/j.jtte.2022.06.001 DOI: https://doi.org/10.1016/j.jtte.2022.06.001
Google Scholar

Circular Economy Action Plan, https://environment.ec.europa.eu/strategy/circular-economy-action-plan_en, available: 15.09.2025
Google Scholar

Jóźwiak-Niedźwiedzka D., Antolik A., Dziedzic K., Lisowski P.: Potential alkaline reactivity of sands from domestic deposits. Roads and Bridges – Drogi i Mosty, 21, 3, 2022, 253-271, DOI: 10.7409/rabdim.022.015 DOI: https://doi.org/10.7409/rabdim.022.015
Google Scholar

Shu X., Huang B.: Recycling of waste tire rubber in asphalt and portland cement concrete: an overview. Construction and Building Materials, 67, Part B, 2014, 217-224, DOI: 10.1016/j.conbuildmat.2013.11.027 DOI: https://doi.org/10.1016/j.conbuildmat.2013.11.027
Google Scholar

Thomas B.S., Gupta R.C.: A comprehensive review on the applications of waste tire rubber in cement concrete. Renewable and Sustainable Energy Reviews, 54, 2016, 1323-1333, DOI: 10.1016/j.rser.2015.10.092 DOI: https://doi.org/10.1016/j.rser.2015.10.092
Google Scholar

Muñoz-Sánchez B., Arévalo-Caballero M.J., Pacheco-Menor M.C.: Influence of acetic acid and calcium hydroxide treatments of rubber waste on the properties of rubberized mortars. Materials and Structures, 50, 75, 2017, 1-16, DOI: 10.1617/s11527-016-0912-7 DOI: https://doi.org/10.1617/s11527-016-0912-7
Google Scholar

Afshinnia K., Poursaee A.: The influence of waste crumb rubber in reducing the alkali-silica reaction in mortar bars. Journal of Building Engineering, 4, 2015, 231-236, DOI: 10.1016/j.jobe.2015.10.002. DOI: https://doi.org/10.1016/j.jobe.2015.10.002
Google Scholar

Huang W., Huang X., Xing Q., Zhou Z.: Strength reduction factor of crumb rubber as fine aggregate replacement in concrete. Journal of Building Engineering, 32, 2020, Article ID: 101346, DOI: 10.1016/j.jobe.2020.101346 DOI: https://doi.org/10.1016/j.jobe.2020.101346
Google Scholar

Turatsinze A., Bonnet S., Granju J.L.: Potential of rubber aggregates to modify properties of cement based-mortars: Improvement in cracking shrinkage resistance. Construction and Building Materials, 21, 1, 2007, 176-181, DOI: 10.1016/j.conbuildmat.2005.06.036 DOI: https://doi.org/10.1016/j.conbuildmat.2005.06.036
Google Scholar

Ling T.C., Nor H.M., Lim S.K.: Using recycled waste tyres in concrete paving blocks. Proceedings of the Institution of Civil Engineers – Waste and Resource Management, 163, 1, 2010, 37-45, DOI: 10.1680/warm.2010.163.1.37 DOI: https://doi.org/10.1680/warm.2010.163.1.37
Google Scholar

Najim K.B., Hall M.R.: Mechanical and dynamic properties of self-compacting crumb rubber modified concrete. Construction and Building Materials, 27, 1, 2012, 521-530, DOI: 10.1016/j.conbuildmat.2011.07.013 DOI: https://doi.org/10.1016/j.conbuildmat.2011.07.013
Google Scholar

Siddique R., Naik T.R.: Properties of concrete containing scrap-tire rubber – an overview. Waste Management, 24, 6, 2004, 563-569, DOI: 10.1016/j.wasman.2004.01.006 DOI: https://doi.org/10.1016/j.wasman.2004.01.006
Google Scholar

Gesoğlu M., Güneyisi E.: Permeability properties of self-compacting rubberized concretes. Construction and Building Materials, 25, 8, 2011, 3319-3326, DOI: 10.1016/j.conbuildmat.2011.03.021 DOI: https://doi.org/10.1016/j.conbuildmat.2011.03.021
Google Scholar

Flores Medina D., Hernández Martínez M.C., Flores Medina N., Hernández-Olivares F.: Durability of rubberized concrete with recycled steel fibers from tyre recycling in aggresive enviroments. Construction and Building Materials, 400, 2023, Article ID: 132619, DOI: 10.1016/j.conbuildmat.2023.132619 DOI: https://doi.org/10.1016/j.conbuildmat.2023.132619
Google Scholar

Abbas S., Ahmed A., Waheed A., Abbas W., Yousaf M., Shaukat S., Alabduljabbar H., Awad Y.A.: Recycled untreated rubber waste for controlling the alkali-silica reaction in concrete. Materials, 15, 10, 2022, Article ID: 3584, DOI: 10.3390/ma15103584 DOI: https://doi.org/10.3390/ma15103584
Google Scholar

Jóźwiak-Niedźwiedzka D., Antolik A.: Assessment of highway pavement concrete suffering from alkali-silica reaction: case study. Materiales de Construcción, 72, 348, 2022, Article ID: e299, DOI: 10.3989/mc.2022.296922 DOI: https://doi.org/10.3989/mc.2022.296922
Google Scholar

Wang J., Guo Z., Yuan Q., Zhang P., Fang H.: Effects of ages on the ITZ microstructure of crumb rubber concrete. Construction and Building Materials, 254, 2020, Article ID: 119329, DOI: 10.1016/j.conbuildmat.2020.119329 DOI: https://doi.org/10.1016/j.conbuildmat.2020.119329
Google Scholar

AASHTO R 80-17 Standard practice for determining the reactivity of concrete aggregates and selecting appropriate measures for preventing deleterious expansion in new concrete construction, Washington 2018, https://img.antpedia.com/standard/files/pdfs_ora/20230616/AASHTO/AASHTO %20R%2080-17.pdf, available: 15.09.2025
Google Scholar

RILEM Recommended Test Method: AAR-2 – Detection of Potential Alkali-Reactivity – Accelerated Mortar-Bar Test Method for Aggregates. In: RILEM Recommendations for the Prevention of Damage by Alkali-Aggregate Reactions in New Concrete Structures. Eds. Nixon P., Sims I., 2016, 61-77 DOI: https://doi.org/10.1007/978-94-017-7252-5_4
Google Scholar

PN-EN 196-1:2016 Methods of Testing Cement – Determination of Strength
Google Scholar

ul Haq Z., Ren T., Yue X., Formela K., Rodrigue D., Colom Fajula X., McNally T., Dawei D., Zhang Y., Wang S.: Progress in devulcanization of waste tire rubber: Upcycling towards a circular economy. Express Polymer Letters, 19, 3, 2025, 258-293, DOI: 10.3144/expresspolymlett.2025.20 DOI: https://doi.org/10.3144/expresspolymlett.2025.20
Google Scholar

Sienkiewicz M., Janik H., Borzędowska-Labuda K., KucińskaLipka J.: Environmentally friendly polymer-rubber composites obtained from waste tyres: A review. Journal of Cleaner Production, 147, 2017, 560-571, DOI: 10.1016/j.jclepro.2017.01.121 DOI: https://doi.org/10.1016/j.jclepro.2017.01.121
Google Scholar

Smith B.C.: The infrared spectra of polymers III: hydrocarbon polymers. Spectroscopy, 36, 11, 2021, 22-25, DOI: 10.56530/spectroscopy.mh7872q7 DOI: https://doi.org/10.56530/spectroscopy.mh7872q7
Google Scholar

Ma Q., Dutta S., Wu K.C.W., Kimura T.: Analytical understanding of the materials design with well‐described shrinkages on multiscale. Chemistry – A European Journal, 24, 2018, 6886-6904, DOI: 10.1002/chem.201704198 DOI: https://doi.org/10.1002/chem.201704198
Google Scholar

Eldin N.N., Senouci A.B.: Rubber‐tire particles as concrete aggregate. Journal of Materials in Civil Engineering, 5, 4, 1993, 478-496, DOI: 10.1061/(ASCE)0899-1561(1993)5:4(478) DOI: https://doi.org/10.1061/(ASCE)0899-1561(1993)5:4(478)
Google Scholar

Khatib Z.K., Bayomy F.M.: Rubberized portland cement concrete. Journal of Materials in Civil Engineering, 11, 3, 1999, 206-213, DOI: 10.1061/(ASCE)0899-1561(1999)11:3(206) DOI: https://doi.org/10.1061/(ASCE)0899-1561(1999)11:3(206)
Google Scholar

Segre N., Joekes I.: Use of tire rubber particles as addition to cement paste. Cement and Concrete Research, 30, 9, 2000, 1421-1425, DOI: 10.1016/S0008-8846(00)00373-2 DOI: https://doi.org/10.1016/S0008-8846(00)00373-2
Google Scholar

Youssf O., ElGawady M.A., Mills J.E., Ma X.: An experimental investigation of crumb rubber concrete confined by fibre reinforced polymer tubes. Construction and Building Materials, 53, 2014, 522-532, DOI: 10.1016/j.conbuildmat.2013.12.007 DOI: https://doi.org/10.1016/j.conbuildmat.2013.12.007
Google Scholar

Daria Jóźwiak-Niedźwiedzka

djozwiak@ippt.pan.pl
https://orcid.org/0000-0003-3681-0817

Affiliation:

Polish Academy of Sciences, Institute of Fundamental Technological Research, 5b Pawińskiego St., 02-106 Warsaw Poland

Dominik Nowicki

https://orcid.org/0009-0009-7159-7880

Affiliation:

Polish Academy of Sciences, Institute of Fundamental Technological Research, 5b Pawińskiego St., 02-106 Warsaw Poland

Piotr Denis

https://orcid.org/0000-0002-1105-3381

Affiliation:

Polish Academy of Sciences, Institute of Fundamental Technological Research, 5b Pawińskiego St., 02-106 Warsaw Poland

Magdalena Osial

https://orcid.org/0000-0003-3076-3415

Affiliation:

Polish Academy of Sciences, Institute of Fundamental Technological Research, 5b Pawińskiego St., 02-106 Warsaw Poland

Alessandro P. Fantilli

https://orcid.org/0000-0003-0383-7191

Affiliation:

Politecnico di Torino, Department of Structural, Building and Geotechnical Engineering, Corso Duca degli Abruzzi 24, 10129 Torino Italy

Influence of granulated rubber from waste tires on ASR expansion, microstructure, and mechanical properties of mortars

Abstract

Keywords:

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Daria Jóźwiak-Niedźwiedzka

Dominik Nowicki

Piotr Denis

Magdalena Osial

Alessandro P. Fantilli